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A simple microwave approach for synthesis and characterization of Ag2S-AgInS2 nanocomposites

Identifieur interne : 000204 ( Main/Repository ); précédent : 000203; suivant : 000205

A simple microwave approach for synthesis and characterization of Ag2S-AgInS2 nanocomposites

Auteurs : RBID : Pascal:14-0102078

Descripteurs français

Pascal (Inist)
- Préparation, Sulfure d'argent, Nanocomposite, Morphologie, Dimension particule, Indium Sulfure, Photoluminescence, Composite matrice métallique, Mécanisme réaction, Traitement thermique, Cellule solaire, Etude expérimentale, Matériau composite, Propriété optique.
Wicri :
- concept : Matériau composite.

English descriptors

KwdEn :
- Composite materials, Experimental study, Heat treatments, Indium Sulfides, Metal matrix composite, Morphology, Nanocomposites, Optical properties, Particle size, Photoluminescence, Preparation, Reaction mechanism, Silver sulfide, Solar cells.

Abstract

Ag₂S-AgInS₂ nanocomposites, with the aid of [Ag(HSal)] and InCl₃ as starting reagents, have been successfully synthesized by a microwave process from propylene glycol solution. Besides, the effects of preparation parameters such as irradiation time, solvents and sulfur source on the morphology and particle size of products were studied by SEM images. The synthesis procedure is novel, simple and uses less toxic reagents. The prepared Ag₂S-AgInS₂ nanostructures were characterized extensively by means of X-ray diffraction (XRD), energy-dispersive X-ray analysis (EDX), scanning electron microscopy (SEM), transmission electron microscopy (TEM), infrared (IR) spectrum, photoluminescence (PL) spectroscopy. The fill factor (FF), open circuit voltage (V_oc), and short circuit current (T_sc) were obtained by I-V characterization.

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Le document en format XML

<record><TEI><teiHeader><fileDesc><titleStmt><title xml:lang="en" level="a">A simple microwave approach for synthesis and characterization of Ag<sub>2</sub>
S-AgInS<sub>2 </sub>
nanocomposites</title>
<author><name sortKey="Mousavi Kamazani, Mehdi" uniqKey="Mousavi Kamazani M">Mehdi Mousavi-Kamazani</name>
<affiliation wicri:level="1"><inist:fA14 i1="01"><s1>Institute of Nano Science and Nano Technology, University of Kashan, P.O. Box 87317-51167</s1>
<s2>Kashan</s2>
<s3>IRN</s3>
<sZ>1 aut.</sZ>
<sZ>2 aut.</sZ>
</inist:fA14>
<country>Iran</country>
<wicri:noRegion>Kashan</wicri:noRegion>
</affiliation>
</author>
<author><name sortKey="Salavati Niasari, Masoud" uniqKey="Salavati Niasari M">Masoud Salavati-Niasari</name>
<affiliation wicri:level="1"><inist:fA14 i1="01"><s1>Institute of Nano Science and Nano Technology, University of Kashan, P.O. Box 87317-51167</s1>
<s2>Kashan</s2>
<s3>IRN</s3>
<sZ>1 aut.</sZ>
<sZ>2 aut.</sZ>
</inist:fA14>
<country>Iran</country>
<wicri:noRegion>Kashan</wicri:noRegion>
</affiliation>
<affiliation wicri:level="1"><inist:fA14 i1="02"><s1>Department of Inorganic Chemistry, Faculty of Chemistry, University of Kashan, P.O. Box 87317-51167</s1>
<s2>Kashan</s2>
<s3>IRN</s3>
<sZ>2 aut.</sZ>
</inist:fA14>
<country>Iran</country>
<wicri:noRegion>Kashan</wicri:noRegion>
</affiliation>
</author>
</titleStmt>
<publicationStmt><idno type="inist">14-0102078</idno>
<date when="2014">2014</date>
<idno type="stanalyst">PASCAL 14-0102078 INIST</idno>
<idno type="RBID">Pascal:14-0102078</idno>
<idno type="wicri:Area/Main/Corpus">000006</idno>
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<seriesStmt><idno type="ISSN">1359-8368</idno>
<title level="j" type="abbreviated">Compos., Part B Eng.</title>
<title level="j" type="main">Composites. Part B, Engineering</title>
</seriesStmt>
</fileDesc>
<profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Composite materials</term>
<term>Experimental study</term>
<term>Heat treatments</term>
<term>Indium Sulfides</term>
<term>Metal matrix composite</term>
<term>Morphology</term>
<term>Nanocomposites</term>
<term>Optical properties</term>
<term>Particle size</term>
<term>Photoluminescence</term>
<term>Preparation</term>
<term>Reaction mechanism</term>
<term>Silver sulfide</term>
<term>Solar cells</term>
</keywords>
<keywords scheme="Pascal" xml:lang="fr"><term>Préparation</term>
<term>Sulfure d'argent</term>
<term>Nanocomposite</term>
<term>Morphologie</term>
<term>Dimension particule</term>
<term>Indium Sulfure</term>
<term>Photoluminescence</term>
<term>Composite matrice métallique</term>
<term>Mécanisme réaction</term>
<term>Traitement thermique</term>
<term>Cellule solaire</term>
<term>Etude expérimentale</term>
<term>Matériau composite</term>
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<front><div type="abstract" xml:lang="en">Ag<sub>2</sub>
S-AgInS<sub>2</sub>
 nanocomposites, with the aid of [Ag(HSal)] and InCl<sub>3</sub>
 as starting reagents, have been successfully synthesized by a microwave process from propylene glycol solution. Besides, the effects of preparation parameters such as irradiation time, solvents and sulfur source on the morphology and particle size of products were studied by SEM images. The synthesis procedure is novel, simple and uses less toxic reagents. The prepared Ag<sub>2</sub>
S-AgInS<sub>2</sub>
 nanostructures were characterized extensively by means of X-ray diffraction (XRD), energy-dispersive X-ray analysis (EDX), scanning electron microscopy (SEM), transmission electron microscopy (TEM), infrared (IR) spectrum, photoluminescence (PL) spectroscopy. The fill factor (FF), open circuit voltage (V<sub>oc</sub>
), and short circuit current (T<sub>sc</sub>
) were obtained by I-V characterization.</div>
</front>
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S-AgInS<sub>2 </sub>
nanocomposites</s1>
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<fA11 i1="01" i2="1"><s1>MOUSAVI-KAMAZANI (Mehdi)</s1>
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<fA14 i1="01"><s1>Institute of Nano Science and Nano Technology, University of Kashan, P.O. Box 87317-51167</s1>
<s2>Kashan</s2>
<s3>IRN</s3>
<sZ>1 aut.</sZ>
<sZ>2 aut.</sZ>
</fA14>
<fA14 i1="02"><s1>Department of Inorganic Chemistry, Faculty of Chemistry, University of Kashan, P.O. Box 87317-51167</s1>
<s2>Kashan</s2>
<s3>IRN</s3>
<sZ>2 aut.</sZ>
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<fC01 i1="01" l="ENG"><s0>Ag<sub>2</sub>
S-AgInS<sub>2</sub>
 nanocomposites, with the aid of [Ag(HSal)] and InCl<sub>3</sub>
 as starting reagents, have been successfully synthesized by a microwave process from propylene glycol solution. Besides, the effects of preparation parameters such as irradiation time, solvents and sulfur source on the morphology and particle size of products were studied by SEM images. The synthesis procedure is novel, simple and uses less toxic reagents. The prepared Ag<sub>2</sub>
S-AgInS<sub>2</sub>
 nanostructures were characterized extensively by means of X-ray diffraction (XRD), energy-dispersive X-ray analysis (EDX), scanning electron microscopy (SEM), transmission electron microscopy (TEM), infrared (IR) spectrum, photoluminescence (PL) spectroscopy. The fill factor (FF), open circuit voltage (V<sub>oc</sub>
), and short circuit current (T<sub>sc</sub>
) were obtained by I-V characterization.</s0>
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<fC02 i1="02" i2="X"><s0>001D06C02D1</s0>
</fC02>
<fC02 i1="03" i2="X"><s0>230</s0>
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<fC03 i1="01" i2="X" l="FRE"><s0>Préparation</s0>
<s5>01</s5>
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<fC03 i1="01" i2="X" l="ENG"><s0>Preparation</s0>
<s5>01</s5>
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<s5>02</s5>
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<fC03 i1="02" i2="X" l="SPA"><s0>Plata sulfuro</s0>
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<s5>03</s5>
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<s5>04</s5>
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<s5>04</s5>
</fC03>
<fC03 i1="05" i2="3" l="FRE"><s0>Dimension particule</s0>
<s5>05</s5>
</fC03>
<fC03 i1="05" i2="3" l="ENG"><s0>Particle size</s0>
<s5>05</s5>
</fC03>
<fC03 i1="06" i2="3" l="FRE"><s0>Indium Sulfure</s0>
<s2>NC</s2>
<s2>NA</s2>
<s5>06</s5>
</fC03>
<fC03 i1="06" i2="3" l="ENG"><s0>Indium Sulfides</s0>
<s2>NC</s2>
<s2>NA</s2>
<s5>06</s5>
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<s5>08</s5>
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<s5>08</s5>
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<s5>08</s5>
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<s5>09</s5>
</fC03>
<fC03 i1="09" i2="X" l="ENG"><s0>Reaction mechanism</s0>
<s5>09</s5>
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<fC03 i1="09" i2="X" l="SPA"><s0>Mecanismo reacción</s0>
<s5>09</s5>
</fC03>
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<s5>10</s5>
</fC03>
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<s5>10</s5>
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<s5>11</s5>
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<fC03 i1="11" i2="3" l="ENG"><s0>Solar cells</s0>
<s5>11</s5>
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<s5>12</s5>
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<s5>31</s5>
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<fC03 i1="13" i2="3" l="ENG"><s0>Composite materials</s0>
<s5>31</s5>
</fC03>
<fC03 i1="14" i2="3" l="FRE"><s0>Propriété optique</s0>
<s5>32</s5>
</fC03>
<fC03 i1="14" i2="3" l="ENG"><s0>Optical properties</s0>
<s5>32</s5>
</fC03>
<fN21><s1>139</s1>
</fN21>
</pA>
</standard>
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A simple microwave approach for synthesis and characterization of Ag2S-AgInS2 nanocomposites

A simple microwave approach for synthesis and characterization of Ag2S-AgInS2 nanocomposites

Descripteurs français

English descriptors

Abstract

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